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By L. S. Bark, S. M. Bark, R. Belcher and H. Freiser (Auth.)

ISBN-10: 008013047X

ISBN-13: 9780080130477

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T . , SEBBORN, W . S . and SELMAN, R . F . W . , Ibid. 8 8 , 7 9 7 , (1963). 2 4 . D E LEO, A . B . , / . Pharm. Sei. 5 4 , 9 1 1 ( 1 9 6 5 ) . 2 5 . PRIESTLEY, P . T . , SEBBORN, W . S . and SELMAN, R . F . W . , Analyst 9 0 , 5 8 9 (1965). 2 6 . PRIESTLEY, P . T . , / . Sei. Instruments 4 2 , 3 5 ( 1 9 6 5 ) . CHAPTER 3 NEUTRALISATION REACTIONS IN AQUEOUS SOLUTIONS I N THE titrimetric study of neutralisation reactions, using for endpoint detection either visual indicators, Potentiometrie or conductiometric methods, analytically acceptable values are only certainly obtained titrating a strong acid against a strong base.

Thus the actual time of titration, viz, the volume of the titrant added, is accurately recorded. APPARATUS 37 In 1965, De Leo and Stern^24) applied the thermometric method to the analysis of pharmaceutical products and described an apparatus whereby the third derivative of the imbalance potential of a suitable Wheatstone bridge was used to indicate the end point of the titration. Observing that a first derivative thermometric titration curve resembles an original Potentiometrie titration curve, the third derivative of a thermometric curve should resemble a second deri­ vative potentiogram in that the end point corresponds to the point where the curve crosses the abscissa after an initial rise, they in­ corporated the control units of a commercially available automatic Potentiometrie titrator into a thermometric titration system.

And REIN, J. , Ibid. 3 0 , 284 (1958). 11. BELL, J. M. and COWELL, C . F . , / . Amer. Soc. 3 5 , 49 (1913). 12. GouDARD, L . , Compt. Rendus 2 6 3 , 10 (1966). 13. POPPER, E . , ROMAN, L . and MARCU, P . , Talanta 1 1 , 515 (1964). 14. VAUGHAN, G . A. and SWITHENBANK, J. , Analyst 9 0 , 594 (1965). 15. PARIS, R . , Chimie Analyt. 3 4 , 3 (1952). 16. PANDYA, P . K . and HALDAR, B . C , / . Sei. Ind. Res. India. Β 2 1 , 503 (1962). 17. POPPER, Ε . , ROMAN, L . and MARCU, P . , Talanta 1 2 , 249 (1965).

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Thermometric Titrimetry by L. S. Bark, S. M. Bark, R. Belcher and H. Freiser (Auth.)


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